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class="rightbot"> </div> <div class="left2top mt10"> </div> <div class="left2_main"> <div class="n_info_con" id="printableview"> <h1> 聚合氯化鋁制備方法簡析</h1> <div class="info_con_tit"> <div class="info_con_tit"> <div class="n_tit"> <span>發表時間：2015-09-22 16:00【<a href="javascript:;" onclick="ChangeFontSize(this,'16px')">大</a> <a class="cur" href="javascript:;" onclick="ChangeFontSize(this,'14px')">中</a> <a href="javascript:;" onclick="ChangeFontSize(this,'12px')">小</a>】</span> </div> </div> </div> <div id="cntrBody"> <p><span style=";font-family:宋體;font-size:14px">聚合氯化鋁的合成方法有很多種，按照原材料的不同，可分為金屬鋁法、活性氫氧化鋁法、三氧化二鋁法、氯化鋁法等。</span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">金屬鋁法</span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">采用金屬鋁法合成聚合氯化鋁的原料主要為鋁加工的下腳料，如鋁屑、鋁灰和鋁渣等。由鋁灰按一定配比在攪拌下緩慢加入鹽酸進行反應，經熟化聚合、沉降制得液體聚合氯化鋁，再經稀釋過濾，濃縮，干燥制得。在工藝上可分為酸法、堿法、中和法<span style="font-family:Times New Roman">3</span><span style="font-family:宋體">種。酸法主要是用</span><span style="font-family:Times New Roman">HCl</span><span style="font-family:宋體">，產品質量不易控制；堿法生產工藝難度較高，設備投資較大且用堿量大，</span><span style="font-family:Times New Roman">pH</span><span style="font-family:宋體">控制費原料，成本較高；用的最多的是中和法，只要控制好配比，一般都能達到國家標準。</span></span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">氫氧化鋁法</span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">氫氧化鋁粉純度比較高，合成的聚合氯化鋁重金屬等有毒物質含量低，一般采用加熱加壓酸溶的生產工藝。這種工藝比較簡單，但生產的聚合氯化鋁的鹽基度較低，因此一般采用氫氧化鋁加溫加壓酸溶再加上鋁酸鈣礦粉中和兩道工序。</span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">三氧化鋁法</span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">含三氧化二鋁的原料主要有三水鋁石、鋁釩土、高嶺土、煤矸石等。該生產工藝可分為兩步：第一步是得到結晶氯化鋁，第二步是通過熱解法或中和法得到聚合氯化鋁；</span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">氯化鋁法</span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">采用氯化鋁粉為原料，加工聚合氯化鋁。這種方法應用最為普遍?？捎媒Y晶氯化鋁于<span style="font-family:Times New Roman">170</span><span style="font-family:宋體">℃進行沸騰熱解，加水熟化聚合，再經固化，干燥制得。</span></span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">堿溶法</span></p><p><span style=";font-family:宋體;font-size:14px"> </span></p><p><span style=";font-family:宋體;font-size:14px">先將鋁灰與氫氧化鈉反應得到鋁酸鈉溶液，再用鹽酸調<span style="font-family:Times New Roman">pH</span><span style="font-family:宋體">值，制得聚合氯化鋁溶液。這種方法的制得的產品顏色外觀較好，水不溶物較少，但氯化鈉含量高，原材料消耗高，溶液氧化鋁含量低，工業化生產成本較大。</span></span></p><p><br/></p> </div> <div class="clear"> </div> <div class="apage" id="showfenye">  <script type="text/javascript"> var pagecont=1; if(pagecont >= 2) { var ss = new Cls_jsPage(1, 1, 5, "ss"); 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